Related Products of 3641-13-2, In the chemical reaction process, reaction time, type of solvent, can easily affect the result of the reaction, thereby determining the yield and properties of the reaction product. An updated downstream synthesis route of 3641-13-2 as follows.
The organometallic complex [Mo(CO)3Br2(NCMe)2] was preparedaccording to literature methods [1,4,5]. A solution of Mo-II(2.3 g, 5.45 mmol) in ethanol (60 mL) was treated with 3-amino-1,2,4-triazole-5-carboxylic acid (ATZAc) (0.70 g, 5.45 mmol). Theresulting solutionwas stirred for 8 h under reflux and evaporated todryness. The solid obtained was washed with hexane and dried under vacuum (2.22 g of yield) [6]. Elemental Analysis forMoC7O3Br2N2H6 (421.94 g/mol): calculated C 19.90%, N 6.63%, H1.42%, Mo 22.73%; found C 19.76%, N 6.59%, H 1.31%, Mo 22.65%. IR(KBr pellet, cm-1): nu (?CO) =1879, 1974, 204, nu (C?O) =1679. EDS(Full scale 37854 ct cursor: -0.348 (octs), keV): C, N, O, Br, Mo.
According to the analysis of related databases, 3641-13-2, the application of this compound in the production field has become more and more popular.
Reference:
Article; Vieira, Eduardo Guimaraes; Dal-Bo, Alexandre Goncalves; Frizon, Tiago Elias Allievi; Dias Filho, Newton Luiz; Journal of Organometallic Chemistry; vol. 834; (2017); p. 73 – 82;,
1,2,3-Triazole – Wikipedia,
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