Research speed reading in 2021. Redox catalysis has been broadly utilized in electrochemical synthesis due to its kinetic advantages over direct electrolysis. 16227-12-6, name is 4-Phenyl-4H-1,2,4-triazole belongs to triazoles compound, it is a common compound, a new synthetic route is introduced below. Recommanded Product: 4-Phenyl-4H-1,2,4-triazole
General procedure: 1,4-bis(Bromomethyl)benzene (0.20 g, 0.76 mmol) and the appropriateimidazole or triazole (1.60 mmol) in DCM (3 mL) were refluxed for 12.16 h in a 10 mL Ace pressure tube. The reaction mixture was cooledto room temperature and extracted with water (3 ~ 5 mL). The aqueousphase was dried in vacuo and the crude product crystallised frommethanol/acetone (1:4) to give pure product as a white solid.
Balanced chemical reaction does not necessarily reveal either the individual elementary reactions by which a reaction occurs or its rate law. In my other articles, you can also check out more blogs about 16227-12-6, and we look forward to future research findings.
Reference:
Article; Du, Yufeng; Tang, Huiling; Ding, Hong; Shi, Yanhui; Cao, Changsheng; Pang, Guangsheng; Journal of Chemical Research; vol. 40; 12; (2016); p. 735 – 739;,
1,2,3-Triazole – Wikipedia,
Triazoles – an overview | ScienceDirect Topics