Research speed reading in 2021. Redox catalysis has been broadly utilized in electrochemical synthesis due to its kinetic advantages over direct electrolysis. 4928-87-4, name is 1,2,4-Triazole-3-carboxylic acid belongs to triazoles compound, it is a common compound, a new synthetic route is introduced below. Computed Properties of C3H3N3O2
To isolate single crystals of [Mn(L)2(H2O)2] (1), 1H-1,2,4-triazole-3-carboxylic acid (0.117 g, 1 mmol), potassium hydroxide (0.04 g, 1 mmol) and manganese(II) chloride tetrahydrate (0.098 g, 0.5 mmol) were placed in the main arm of a branched tube to be heated. Water was carefully added to fill both arms, and then the arm to be heated was placed in a bath at 60 C. After 10 days, colorless crystals were deposited in the cooler arm which were filtered off, washed with water and air dried. (0.161 g, yield 51.3%), m.p. > 300 C.
The catalyzed pathway has a lower Ea, but the net change in energy that results from the reaction is not affected by the presence of a catalyst. In my other articles, you can also check out more blogs about 4928-87-4
Reference:
Article; Safarifard, Vahid; Morsali, Ali; Ultrasonics Sonochemistry; vol. 21; 1; (2014); p. 253 – 261;,
1,2,3-Triazole – Wikipedia,
Triazoles – an overview | ScienceDirect Topics