Application of 1455-77-2

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Adding a certain compound to certain chemical reactions, such as: 1455-77-2, name is 3,5-Diamino-1,2,4-triazole, belongs to triazoles compound, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 1455-77-2, HPLC of Formula: C2H5N5

3,5-Diamino-1,2,4-triazole was loaded into crystallization vessel inside a dry box. aHF (5?10 ml) was condensed onto the solid at 77 K and the reaction mixture was brought to ambient temperature. The resulting clear solution was decanted into the 6-mm o.d. side arm. Evaporation of the solvent from this solution was carried out by maintaining a temperature gradient of ca. 10?20 ¡ãC between both tubes for several weeks. Slow distillation of aHF from the 6-mm o.d. tube into the 19-mm o.d. tube resulted in growth of crystals compound II inside the 6-mm o.d. tube.

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Reference:
Article; Goreshnik, Evgeny; Journal of Fluorine Chemistry; vol. 197; (2017); p. 94 – 99;,
1,2,3-Triazole – Wikipedia,
Triazoles – an overview | ScienceDirect Topics