107534-96-3 - | Triazoles

15-Sep-21 News A new synthetic route of 107534-96-3

I hope this article can help some friends in scientific research. I am very proud of our efforts over the past few months and hope to 3-((1H-1,2,4-Triazol-1-yl)methyl)-1-(4-chlorophenyl)-4,4-dimethylpentan-3-ol help many people in the next few years.

New discoveries in chemical research and development in 2021. The transformation of simple hydrocarbons into more complex and valuable products via catalytic C–H bond functionalisation has revolutionised modern synthetic chemistry. 107534-96-3, name is 3-((1H-1,2,4-Triazol-1-yl)methyl)-1-(4-chlorophenyl)-4,4-dimethylpentan-3-ol belongs to triazoles compound, it is a common compound, a new synthetic route is introduced below. Safety of 3-((1H-1,2,4-Triazol-1-yl)methyl)-1-(4-chlorophenyl)-4,4-dimethylpentan-3-ol

Complex trans-[PdCl2L2] (I) was prepared at 20by methods A and B at different predetermined Pd(II):L molar ratios. Method A: The batch ratio was Pd(II) : L = 1 : 2.To a magnetically stirred aqueous solution (3 mL) containing K2[PdCl4] (0.30 g, 0.92 mmol), the reagent L (0.57 g, 1.84 mmol) dissolved in acetone (6.5 mL)was added. The brown color of the solution quickly changed to orange. The bulky yellow precipitate was formed in 5 h; in 16 h after the evaporation of acetone,the precipitate was filtered out, washed with water and then hexane, and dried in air. The yield was 97%. Method B: The predetermined ratio was Pd(II) : L =1 : 1. To an aqueous solution (3 mL) containing K2[PdCl4] (0.30 g, 0.92 mmol), the reagent (0.28 g,0.92 mmol) dissolved in acetone (6.5 mL) was added under stirring. A yellow precipitate was formed in few minutes. After stirring for 24 h the precipitate was filtered out, washed with water and hexane, and dried. The yield was 81% based on the reagent.

Reference:
Article; Khisamutdinov; Shitikova; Anpilogova; Golubyatnikova; Mulagaleev; Murinov; Russian Journal of Inorganic Chemistry; vol. 60; 5; (2015); p. 638 – 646; Zh. Neorg. Khim.; vol. 60; 5; (2015); p. 710 – 718,9;,
1,2,3-Triazole – Wikipedia,
Triazoles – an overview | ScienceDirect Topics

9/6/21 News Chemical Properties and Facts of 107534-96-3

I am very proud of our efforts over the past few months and hope to 3-((1H-1,2,4-Triazol-1-yl)methyl)-1-(4-chlorophenyl)-4,4-dimethylpentan-3-ol help many people in the next few years.

Electric Literature of 107534-96-3, New Advances in Chemical Research in 2021.In classical electrochemical theory, both the electron transfer rate and the adsorption of reactants at the electrode control the electrochemical reaction. 107534-96-3, name is 3-((1H-1,2,4-Triazol-1-yl)methyl)-1-(4-chlorophenyl)-4,4-dimethylpentan-3-ol, molecular formula is C16H22ClN3O, its traditional synthetic route has been very mature, but the traditional synthetic route has various shortcomings, below Introduce a new synthetic route.

First, tebuconazole (184 mg, 0.6 mmol) was dissolved in anhydrous dichloromethaneIn (CH2Cl2, 15 mL), add triethylamine(C6H15N, 730 mg, 7.2 mmol), after stirring in an ice bath for 5 minutes,Addition of monoethylmonosuccinate (C6H9ClO3, 988 mg, 6 mmol)Stir overnight at room temperature, followed by washing with water and saturated saline(15 mL×3, respectively), after drying the dichloromethane with anhydrous sodium sulfate,It was filtered, evaporated to dryness under reduced pressure to give the intermediate product (about 400 mg).Used directly for the next hydrolysis. The product structure was characterized by LC/MS.

I am very proud of our efforts over the past few months and hope to 3-((1H-1,2,4-Triazol-1-yl)methyl)-1-(4-chlorophenyl)-4,4-dimethylpentan-3-ol help many people in the next few years.

Reference:
Patent; Henan University of Science and Technology; Chen Xiujin; Li Zhaozhou; Wang Yao; Gao Hongli; Li Zhili; Cao Li; Li Daomin; Xu Chuanlai; (16 pag.)CN106674138; (2017); A;,
1,2,3-Triazole – Wikipedia,
Triazoles – an overview | ScienceDirect Topics

Research on new synthetic routes about 107534-96-3

Sometimes chemists are able to propose two or more mechanisms that are consistent with the available data. If a proposed mechanism predicts the wrong experimental rate law, however, the mechanism must be incorrect.Welcome to check out more blogs about 3-((1H-1,2,4-Triazol-1-yl)methyl)-1-(4-chlorophenyl)-4,4-dimethylpentan-3-ol, in my other articles.

Research speed reading in 2021. In classical electrochemical theory, both the electron transfer rate and the adsorption of reactants at the electrode control the electrochemical reaction. 107534-96-3, name is 3-((1H-1,2,4-Triazol-1-yl)methyl)-1-(4-chlorophenyl)-4,4-dimethylpentan-3-ol belongs to triazoles compound, it is a common compound, a new synthetic route is introduced below. Application In Synthesis of 3-((1H-1,2,4-Triazol-1-yl)methyl)-1-(4-chlorophenyl)-4,4-dimethylpentan-3-ol

The complex was synthesized by two methods. To an aqueous solution (3 mL) containing Na2[PtCl6]*6H2O (0.50 g, 0.89 mmol), reagent L (0.27 g, 0.89 mmol) (method A) or (0.55 g, 1.78 mmol) (method B) in acetone (7 mL) was added under stirring. A yellow precipitate was quickly formed. After 72 h, the precipitate was filtered out, washed with water and hexane, and dried in air. The yield based on reagent L was 67% (method A) and 90% (method B).

Reference:
Article; Khisamutdinov; Anpilogova; Shitikova; Murinov, Yu. I.; Russian Journal of Inorganic Chemistry; vol. 61; 12; (2016); p. 1530 – 1537; Zh. Neorg. Khim.; vol. 61; 12; (2016); p. 1591 – 1598,8;,
1,2,3-Triazole – Wikipedia,
Triazoles – an overview | ScienceDirect Topics

The Shocking Revelation of Application of 107534-96-3

The potential utility of systematic synthetic strategy will be applicable to efficient generations of chemical libraries of compounds to find ‘hit’ molecules.Read on for other articles about 3-((1H-1,2,4-Triazol-1-yl)methyl)-1-(4-chlorophenyl)-4,4-dimethylpentan-3-ol, hurry up and to see.

Electric Literature of 107534-96-3, New Advances in Chemical Research in 2021. The transformation of simple hydrocarbons into more complex and valuable products via catalytic C–H bond functionalisation has revolutionised modern synthetic chemistry. 107534-96-3, name is 3-((1H-1,2,4-Triazol-1-yl)methyl)-1-(4-chlorophenyl)-4,4-dimethylpentan-3-ol, molecular formula is C16H22ClN3O, its traditional synthetic route has been very mature, but the traditional synthetic route has various shortcomings, below Introduce a new synthetic route.

Example 8 Synthesis of 2-{2-[2-(4-chloro-phenyl)-ethyl]-2-hydroxy-3,3-dimethyl-butyl}- 2,4-dihydro-[1 ,2,4]triazole-3-thioneTo an ice-cold solution of 1 -(4-chloro-phenyl)-4,4-dimethyl-3-[1 ,2,4]triazol-1 -ylmethyl- pentan-3-ol (236 mg, 0.77 mmol) in 2 mL of THF was added a solution iPrMgCI in THF (2.0 M, 1 .0 mL, 2.0 mmol). The solution was warmed to 40 C and kept at that temperature for 90 min. Then, it was cooled to 0 C and treated and a suspension of sulfur (75 g, 2.34 mmol) in 1 mL of THF was added portionwise and the mixture stirred for another 60 min at 0 C. The solution was then poured onto 4% HCI (20 mL). The a- queous phase was extracted with TBME (2×30 mL). The combined org. phases were successively washed with water and brine. The crude product was obtained after drying over Na2S04 and removal of all volatiles. Purification was accomplished through flash column chromatography on silica (cyclohexane/EtOAc mixtures) to obtain the product as a colorless liquid (151 mg, 0.44 mmol, 58% yield).1H N R (DMSO-de. 500 MHz): delta (ppm) = 8.40 (s, 1 H); 7.29 (d, J = 12.0 Hz, 2 H); 7.18 (d, J = 12.0 Hz, 2 H); 4.51 -4.58 (m, 2 H); 4.00-4.06 (m, 1 H); 2.61 (dt, J = 5.0 Hz, J = 17.0 Hz, 1 H); 2.20-2.30 (m, 1 H); 1 .94-2.04 (m, 1 H); 1 .70 (dt, J = 5.0 Hz, J = 19.0 Hz, 1 H); 0.94 (s, 9 H).

Reference:
Patent; BASF SE; DOCHNAHL, Maximilian; KEIL, Michael; GEBHARDT, Joachim; VOGELBACHER, Uwe Josef; MENGES, Frederik; RACK, Michael; RENNER, Jens; WOLF, Bernd; WO2011/113820; (2011); A1;,
1,2,3-Triazole – Wikipedia,
Triazoles – an overview | ScienceDirect Topics

What I Wish Everyone Knew About 3-((1H-1,2,4-Triazol-1-yl)methyl)-1-(4-chlorophenyl)-4,4-dimethylpentan-3-ol

Photocatalytic experiments were performed in a photochemical reactor Suntest XLS+ solar simulator (Atlas, Germany) equippedwith a vapor xenon lamp (2.2 kW). The light source was jackedwith special glass filters restricting the transmission of wave-lengths below 290 nm. A Pyrex reactor with a total volume of250 mL was used to study the photocatalytic degradation of TEB.Suspensions of TEB solutions containing different amounts of theTiO2photocatalyst were stirred in the dark for 30 min to achieveadsorption-desorption equilibrium. After this period, the light wasturned on for the photocatalytic degradation experiments.As the reaction progressed, aliquots were withdrawn fromthe reactor at specific time intervals and filtered through HVLP(0.45 m) filters supplied by Millipore to remove TiO2 particlesbefore further analysis. Adsorption and photolytic experiments were also conducted. TEB solutions were prepared in ultrapurewater and wastewaters and the experiments were performed at room temperature

Reference:
Article; Stamatis; Antonopoulou; Konstantinou; Catalysis Today; vol. 252; (2015); p. 93 – 99;,
1,2,3-Triazole – Wikipedia,
Triazoles – an overview | ScienceDirect Topics

Continuously updated synthesis method about 107534-96-3

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Application of 107534-96-3, New discoveries in chemical research and development in 2021. We’ll be discussing some of the latest developments in chemical about CAS: 107534-96-3, name is 3-((1H-1,2,4-Triazol-1-yl)methyl)-1-(4-chlorophenyl)-4,4-dimethylpentan-3-ol, its traditional synthetic route has been very mature, but the traditional synthetic route has various shortcomings, such as complicated route, low yield, poor purity, etc, below Introduce a new synthetic route.

EXAMPLE 2 Preparation of 1-Tert-butyl-3-(p-chlorophenyl)-1-(1H-1,2,4-triazol-1-ylmethyl)propyl diphenylborinate STR11 A solution of diphenylborinic acid (0.11 g, 0.60 mmol) in toluene is added to a solution of 1-(4-chlorophenyl)-4,4-dimethyl-3-(1H-1,2,4-triazol-1-ylmethyl)pentan-3-ol (0.21 g, 0.68 mmol) in a 1:1 ether/toluene solution. The reaction mixture is heated at reflux for 3 days with removal of water (Dean Stark), cooled and concentrated in vacuo to obtain a residue. The residue is chromatographed using silica gel and hexane/ethyl acetate solutions to give the title product as a pale yellow solid, mp 197 C.

We very much hope you enjoy reading the articles and that you will join us to present your own research about 107534-96-3, Happy reading!

Reference:
Patent; American Cyanamid Company; US5591726; (1997); A;,
1,2,3-Triazole – Wikipedia,
Triazoles – an overview | ScienceDirect Topics

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New discoveries in chemical research and development in 2021. The dynamic chemical diversity of the numerous elements, ions and molecules that constitute the basis of life provides wide challenges and opportunities for research. 107534-96-3, name is 3-((1H-1,2,4-Triazol-1-yl)methyl)-1-(4-chlorophenyl)-4,4-dimethylpentan-3-ol belongs to triazoles compound, it is a common compound, a new synthetic route is introduced below. Quality Control of 3-((1H-1,2,4-Triazol-1-yl)methyl)-1-(4-chlorophenyl)-4,4-dimethylpentan-3-ol

For a 1 :1 co-crystal of tebuconazol and 4-hydroxy benzoic acid, 200,1 mg of tebucona- zol, 80,4 mg of 4-hydroxi benzoic acid and 150 muIota ethanol was grinded in a ball mill (Retsch Modell MM301 ) for 10 minutes by using 20 Hz. The crystalline product gave the PXRD in Figure 3 (table 5).

If you are hungry for even more, make sure to check my other article about 107534-96-3, the application of this compound in the production field has become more and more popular.

Reference:
Patent; BASF SE; SAXELL, Heidi, Emilia; ISRAELS, Rafel; SCHAeFER, Ansgar; BRATZ, Matthias; HOeFFKEN, Hans, Wolfgang; BRODE, Ingo; NAUHA, Elisa; NISSINEN, Maija; WO2011/54741; (2011); A2;,
1,2,3-Triazole – Wikipedia,
Triazoles – an overview | ScienceDirect Topics

Discover the magic of the Reference of 107534-96-3

I am very proud of our efforts over the past few months and hope to 3-((1H-1,2,4-Triazol-1-yl)methyl)-1-(4-chlorophenyl)-4,4-dimethylpentan-3-ol help many people in the next few years.

Reference of 107534-96-3, New Advances in Chemical Research in 2021. Chemo-enzymatic cascade processes are invaluable due to their ability to rapidly construct high-value products from available feedstock chemicals in a one-pot relay manner. 107534-96-3, name is 3-((1H-1,2,4-Triazol-1-yl)methyl)-1-(4-chlorophenyl)-4,4-dimethylpentan-3-ol, molecular formula is C16H22ClN3O, its traditional synthetic route has been very mature, but the traditional synthetic route has various shortcomings, below Introduce a new synthetic route.

A portion of cis-[PtCl2(DMSO)2] (0.53 g, 1.26 mmol) placed into a pear-shaped flask of 100 mL in volume was dissolved in chloroform (20 mL) under stirring on a water bath (40C). To the resulting solution, reagent L (0.89 g, 2.89 mmol) was added. The formed light-yellow transparent solution was boiled on a water bath for 19 h under reflux and magnetically stirring and then transferred into a 150-mL beaker and evaporated one-half. Complex I was precipitated from the solution cooled to room temperature with hexane. The mixture of the precipitate and the mother solution was cooled to 10C, the solution was then decanted, and hexane (100 mL) was added to the precipitate, thereupon the mixture was allowed to stand at -10C for 15 h. The precipitate was twice washed with hexane, reprecipitated with hexane from a chloroform solution, filtered out, washed with hexane, and dried in air. The yield was 62%.

I am very proud of our efforts over the past few months and hope to 3-((1H-1,2,4-Triazol-1-yl)methyl)-1-(4-chlorophenyl)-4,4-dimethylpentan-3-ol help many people in the next few years.

What I Wish Everyone Knew About 107534-96-3

Reference of 107534-96-3, New Advances in Chemical Research in 2021. The dynamic chemical diversity of the numerous elements, ions and molecules that constitute the basis of life provides wide challenges and opportunities for research. 107534-96-3, name is 3-((1H-1,2,4-Triazol-1-yl)methyl)-1-(4-chlorophenyl)-4,4-dimethylpentan-3-ol, molecular formula is C16H22ClN3O, its traditional synthetic route has been very mature, but the traditional synthetic route has various shortcomings, below Introduce a new synthetic route.

To an aqueous solution (3 mL) containing K2[PtCl4] (0.30 g, 0.72 mmol), reagent L (0.22 g, 0.72 mmol) in acetone (7 mL) was added under stirring. After 48 h, the settled bulky light-yellow precipitate was filtered out, sequentially washed with water and hexane, and dried in air. The yield based on reagent L was 91%.