Category: 68744-64-9

Simple exploration of 68744-64-9

By the way, if you are interested in learning more fun chemistry with your kids, get your hands into one chemistry set now, and start enjoying the best part of chemistry: experiments about 5-(Trifluoromethyl)-4H-1,2,4-triazole-3-thiol.

Reference of 68744-64-9, New Advances in Chemical Research in 2021.Reactions catalyzed within inorganic and organic materials and at electrochemical interfaces commonly occur at high coverage and in condensed media, 68744-64-9, name is 5-(Trifluoromethyl)-4H-1,2,4-triazole-3-thiol, molecular formula is C3H2F3N3S, its traditional synthetic route has been very mature, but the traditional synthetic route has various shortcomings, below Introduce a new synthetic route.

5-Trifluoromethyl-lH- (1, 2,4)-triazole-3-thiol (l. 0g), heptafluoro-l-iodopropane (3.5 g) and triethyl- amine (0.90 g) were stirred in DMF (10 ml) at 90 C for 24 hours. After cooling to room temperature, he reaction mixture was diluted with ethyl acetate and washed with water and saturated aqueous solution of sodium chloride. After drying the organic layer with magnesium sulfate, the solvent was distilled off under the reduced pressure to obtain 3-heptafluoropropylsulfanyl-5-trifluoro- methyl-lH- (1, 2,4)-triazole (0.70g).

By the way, if you are interested in learning more fun chemistry with your kids, get your hands into one chemistry set now, and start enjoying the best part of chemistry: experiments about 5-(Trifluoromethyl)-4H-1,2,4-triazole-3-thiol.

Reference:
Patent; BAYER CROPSCIENCE AG; WO2005/95351; (2005); A1;,
1,2,3-Triazole – Wikipedia,
Triazoles – an overview | ScienceDirect Topics

Introduction of a new synthetic route about 68744-64-9

The synthetic route of 68744-64-9 has been constantly updated, and we look forward to future research findings.

Application of 68744-64-9, These common heterocyclic compound, 68744-64-9, name is 5-(Trifluoromethyl)-4H-1,2,4-triazole-3-thiol, its traditional synthetic route has been very mature, but the traditional synthetic route has various shortcomings, such as complicated route, low yield, poor purity, etc, below Introduce a new synthetic route.

5-Trifluoromethyl-lH- (1, 2,4)-triazole-3-thiol (l. 0g), heptafluoro-l-iodopropane (3.5 g) and triethyl- amine (0.90 g) were stirred in DMF (10 ml) at 90 C for 24 hours. After cooling to room temperature, he reaction mixture was diluted with ethyl acetate and washed with water and saturated aqueous solution of sodium chloride. After drying the organic layer with magnesium sulfate, the solvent was distilled off under the reduced pressure to obtain 3-heptafluoropropylsulfanyl-5-trifluoro- methyl-lH- (1, 2,4)-triazole (0.70g).

The synthetic route of 68744-64-9 has been constantly updated, and we look forward to future research findings.

Reference:
Patent; BAYER CROPSCIENCE AG; WO2005/95351; (2005); A1;,
1,2,3-Triazole – Wikipedia,
Triazoles – an overview | ScienceDirect Topics