Electric Literature of 13423-60-4, In the chemical reaction process, reaction time, type of solvent, can easily affect the result of the reaction, thereby determining the yield and properties of the reaction product. An updated downstream synthesis route of 13423-60-4 as follows.
EXAMPLE 115 1-phenyl-4-(undec-1-yl)triazolium bromide 0.300 g (0.002 mol) 1-phenyltriazole 1 and 1.41 g (0.006 mol) 1-bromoundecane 2 are combined in a pressure tube. The reaction mixture is stirred for 24 h at 110 C. The reaction mixture is cooled down and the same volume petroleum ether is added. The precipitated solid is filtered off, washed with petroleum ether/THF (1:1), and is dried in HV. M 380.37 C19H30N3N3Br Yield: 0.281 g (37%) 1H-NMR DM-187 (300 MHz/DMSO):
According to the analysis of related databases, 13423-60-4, the application of this compound in the production field has become more and more popular.
Reference:
Patent; TECHNISCHE UNIVERSITAET DRESDEN; US2011/105761; (2011); A1;,
1,2,3-Triazole – Wikipedia,
Triazoles – an overview | ScienceDirect Topics