4928-87-4, As we all know, there are many different methods for the synthesis of a compound, and people can choose the synthesis method that suits their own laboratory according to the actual situation. 4928-87-4 name is 1,2,4-Triazole-3-carboxylic acid, This compound is widely used in many fields, so it is necessary to find a new synthetic route. The downstream synthesis method of this compound is introduced below.
To prepare nano-sized [Mn(L)2(H2O)2] (1), 50ml solution of manganese(II) chloride tetrahydrate (0.1molL-1) in water was positioned in a high-density ultrasonic probe, operating at 40kHz with a maximum power output of 305W. Into this solution water a 50ml solution of the ligand 1H-1,2,4-triazole-3-carboxylic acid (0.1molL-1) and potassium hydroxide (0.01molL-1) were added dropwise. The obtained precipitates were filtered off, washed with water and then dried in air. m.p.>300C.
At the same time, in my other blogs, there are other synthetic methods of this type of compound, 1,2,4-Triazole-3-carboxylic acid, and friends who are interested can also refer to it.
Reference:
Article; Safarifard, Vahid; Morsali, Ali; Ultrasonics Sonochemistry; vol. 21; 1; (2014); p. 253 – 261;,
1,2,3-Triazole – Wikipedia,
Triazoles – an overview | ScienceDirect Topics