1455-77-2, name is 3,5-Diamino-1,2,4-triazole, belongs to Triazoles compound, is considered to be a conventional heterocyclic compound, which is widely used in drug synthesis. The chemical synthesis route is as follows. category: Triazoles
A mixture of Zn(NO3)2?6H2O (0.029 g, 0.10 mmol), Hnic(0.036 g,0.10 mmol), Hdatrz (0.01 g, 0.1 mmol), H2O (2 mL), andDMF (2 mL) was placed in a small vial. The resulting mixture was stirred for 30 min at room temperature, and thenthe mixture was kept at 110C for three days. After beingslowly cooled to the room temperature, colorless block crystals of 1were isolated in 35percent yield based on Zn(II). Anal. Calcd. for C16H16N12O4Zn2(571.19): C, 33.61; N, 29.41; H,2.80percent. Found: C, 33.62; N, 29.38; H, 2.84percent.
The synthetic route of 1455-77-2 has been constantly updated, and we look forward to future research findings.
Reference:
Article; Bu, Xianzhong; Chen, Jinquan; Hu, Mingzhen; Synthesis and Reactivity in Inorganic, Metal-Organic, and Nano-Metal Chemistry; vol. 46; 1; (2016); p. 123 – 126;,
1,2,3-Triazole – Wikipedia,
Triazoles – an overview | ScienceDirect Topics