7343-34-2, In the next few decades, the world population will flourish. As the population grows rapidly and people all over the world use more and more resources, all industries must consider their environmental impact. 7343-34-2, name is 3,5-Dimethyl-4H-1,2,4-triazole belongs to Triazoles compound, it is a common compound, a new synthetic route is introduced below.
A mixture of Zn(NO3)2¡¤6H2O (60 mg, 0.2 mmol), HCOONa¡¤2H2O (14 mg, 0.1 mmol), Hdmtz(19 mg, 0.2 mmol), an aqueous dimethylamine solution (0.3 mmol, 33percent), and H2O (3 ml) was placed in a Teflon-linedstainless steel vessel (12 ml), heated at 120 ¡ãC for 72 h, and then cooled to room temperature at a rate of 5 ¡ãC/h. Colorlessblock crystals of 1 were collected by filtration, washed with water, and dried in air to afford 22 mg (62percent based on Zn) of theproduct. Anal. calcd. for C13H22N10O8Zn4 (percent): C 22.06, H 3.13, N 19.79. Found (percent): C 22.12, H 3.09, N, 19.82. IR(KBr, cm?1): 3476(m), 1612(s), 1527(m), 1451(m), 1385(m), 1340(m), 1129(w), 1036(w), 881(w), 772(w), 700(w), 546(m).
The synthetic route of 3,5-Dimethyl-4H-1,2,4-triazole has been constantly updated, and we look forward to future research findings.
Reference:
Article; Fang; Yang; Dou; Zhu; Xu; Journal of Structural Chemistry; vol. 59; 6; (2018); p. 1450 – 1455; Zh. Strukt. Kim.; vol. 59; 6; (2018); p. 1503 – 1507,5;,
1,2,3-Triazole – Wikipedia,
Triazoles – an overview | ScienceDirect Topics