Adding a certain compound to certain chemical reactions, such as: 10570-40-8, name is 4-Methyl-4H-1,2,4-triazole, belongs to Triazoles compound, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 10570-40-8, COA of Formula: C3H5N3
A solution of 4-methyl-1,2,4-triazole (0.32 g, 3.9 mmol) and benzyl bromide (0.50 mL, 1.1 equiv.) in CH3CN (5 mL) was refluxed for 21 h. On cooling, the product crystallized and was collected by filtration and dried. Yield: 0:72 g (74%). M. p. 158 C. – 1H NMR (300 MHz, [D6]DMSO): delta = 3:91 (s, 3H), 5.66 (s, 2H), 7.38 – 7.43 (m, 5H), 9.21 (s, 1H), 10.32 (s, 1H) ppm. – 13C NMR (75 MHz, [D6]DMSO): delta = 34:2, 54.5, 128.8 (5C), 133.4, 143.2, 145:8 ppm. – IR (neat): nu = 2988 w, 2940 w, 1582 m, 1457 w, 1357 w, 1152 m, 999 w, 912 w, 721 s, 695 s, 640 m, 621 m, 614 m cm-1.
In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles, 4-Methyl-4H-1,2,4-triazole, other downstream synthetic routes, hurry up and to see.
Reference:
Article; Laus, Gerhard; Kahlenberg, Volker; Wurst, Klaus; Schottenberger, Herwig; Zeitschrift fur Naturforschung – Section B Journal of Chemical Sciences; vol. 69; 9-10; (2014); p. 950 – 964;,
1,2,3-Triazole – Wikipedia,
Triazoles – an overview | ScienceDirect Topics