In the chemical reaction process, reaction time, type of solvent, can easily affect the result of the reaction, thereby determining the yield and properties of the reaction product. An updated downstream synthesis route of 4928-87-4 as follows. 4928-87-4
To prepare the nanoparticles of 1, 50ml solution of lead(II) nitrate (0.01 M) in water was positioned in a high-density ultrasonic probe, operating at 40 kHz with a maximum power output of 305 W. Into this aqueous solution a 50 ml solution of the ligand 1H-1,2,4-triazole-3-carboxylic acid (0.01 M) and sodium hydroxide (0.01 M) and potassium bromide (0.01 M) were added dropwise. The obtained precipitates were filtered off, washed with water and then dried in air. m.p.?180 C. (Found C 8.61, H 0.89, N 10.12%). IR (cm-1) selected bands: 466 (s), 661 (s), 1106 (s), 1309 (m), 1373 (m), 1465 (vs), 1610 (s) and 3373 (br).
According to the analysis of related databases, 4928-87-4, the application of this compound in the production field has become more and more popular.
Reference:
Article; Safarifard, Vahid; Morsali, Ali; Joo, Sang Woo; Ultrasonics Sonochemistry; vol. 20; 5; (2013); p. 1254 – 1260;,
1,2,3-Triazole – Wikipedia,
Triazoles – an overview | ScienceDirect Topics