Synthetic Route of 107534-96-3, Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 107534-96-3, name is 3-((1H-1,2,4-Triazol-1-yl)methyl)-1-(4-chlorophenyl)-4,4-dimethylpentan-3-ol, This compound has unique chemical properties. The synthetic route is as follows.
Complex [Pd2Cl4L2] (III) was synthesized at a predetermined ratio Pd(II) : L = 1 : 1. To palladium(II)chloride (0.20 g, 1.13 mmol) placed into a 25mL pear-shaped flask with a reflux condenser, acetonitrile(10 mL) was added, and the resulting mixture was refluxed on a sand bath until the salt was completely dissolved. The formed yellow-brown trans-(bisacetonitrile)dichloropalladium solution was cooled to 60, there upon reagent L (0.35 g, 1.13 mmol) was added. The color of the solution changed to light yellow. Acetonitrile was removed on a rotary evaporator, and the separated substance was washed with hexane and dried. The yield was 95%.
The chemical industry reduces the impact on the environment during synthesis 3-((1H-1,2,4-Triazol-1-yl)methyl)-1-(4-chlorophenyl)-4,4-dimethylpentan-3-ol. I believe this compound will play a more active role in future production and life.
Reference:
Article; Khisamutdinov; Shitikova; Anpilogova; Golubyatnikova; Mulagaleev; Murinov; Russian Journal of Inorganic Chemistry; vol. 60; 5; (2015); p. 638 – 646; Zh. Neorg. Khim.; vol. 60; 5; (2015); p. 710 – 718,9;,
1,2,3-Triazole – Wikipedia,
Triazoles – an overview | ScienceDirect Topics