Research speed reading in 2021. In classical electrochemical theory, both the electron transfer rate and the adsorption of reactants at the electrode control the electrochemical reaction. 7411-23-6, name is 3,5-Dibromo-1H-1,2,4-triazole belongs to triazoles compound, it is a common compound, a new synthetic route is introduced below. Recommanded Product: 7411-23-6
Intermediate 7 l-Benzyl-3,5-dibromo-lH-l,2,4-triazole Sodium te/t-butoxide (932 mg, 9.70 mmol) was added to a solution of 3,5-dibromo-l/-/-l,2,4- triazole (2.0 g, 8.82 mmol) in DMF (15 mL) and stirred at rt for 10 minutes. Benzyl bromide (1.15 mL, 9.70 mmol) was added and the mixture was stirred at rt overnight. Water (100 mL) was added and the mixture was extracted with EtOAc (2 x 50 mL). The organic phase was washed with brine (50 mL), dried over sodium sulfate, and concentrated to give the title compound as a liquid (2.69 g, 96%). XH NMR (400 MHz, CDCI3): delta ppm 5.30 (s, 2 H), 7.29 – 7.39 (m, 5 H).
Sometimes chemists are able to propose two or more mechanisms that are consistent with the available data. If a proposed mechanism predicts the wrong experimental rate law, however, the mechanism must be incorrect.Welcome to check out more blogs about 3,5-Dibromo-1H-1,2,4-triazole, in my other articles.
Reference:
Patent; ACTURUM LIFE SCIENCE AB; BESIDSKI, Yevgeni; YNGVE, Ulrika; PAULSEN, Kim; LINDE, Christian; MALMBORG, Jonas; WO2014/195322; (2014); A1;,
1,2,3-Triazole – Wikipedia,
Triazoles – an overview | ScienceDirect Topics