Application of 74205-82-6, New Advances in Chemical Research in 2021. The prevalence of solvent effects in heterogeneous catalysis in condensed media has motivated developing quantitative kinetic,A common heterocyclic compound, 74205-82-6, name is (1H-1,2,4-Triazol-1-yl)methanol, molecular formula is C3H5N3O, its traditional synthetic route has been very mature, but the traditional synthetic route has various shortcomings, below Introduce a new synthetic route.
General procedure: A mixture containing 25 ml of acetonitrile, two equivalents of (3,5-dimethyl-1H-pyrazol-1-yl) methanol (compound 2), and one equivalent of N,N-Diethyl-propanediamine was stirred at room temperature for 4 days. Next, the solvent was concentrated at a reduced pressure, washed with brine and dichloromethane. The organic solution was dried with MgSO4, and the solvent was concentrated at reduced pressure to yield compound 3 as light yellow oil.
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Article; Bendaha, Hasnae; Yu, Lisa; Touzani, Rachid; Souane, Rachid; Giaever, Guri; Nislow, Corey; Boone, Charles; El Kadiri, Sghir; Brown, Grant W.; Bellaoui, Mohammed; European Journal of Medicinal Chemistry; vol. 46; 9; (2011); p. 4117 – 4124;,
1,2,3-Triazole – Wikipedia,
Triazoles – an overview | ScienceDirect Topics