The origin of a common compound about 7411-23-6

In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles, 7411-23-6, other downstream synthetic routes, hurry up and to see.

A common compound: 7411-23-6, name is 3,5-Dibromo-1H-1,2,4-triazole, belongs to Triazoles compound, it can change the direction of chemical reaction, and react with certain compounds to generate new functional products. A new synthetic method of this compound is introduced below. 7411-23-6

a 3,5-Dibromo-1-(4-methoxyphenylmethyl)-1H-1,2,4-triazole 4-Methoxyphenylmethyl chloride (4.47 ml) was added to a stirred solution of 3,5-dibromo-1,2,4-triazole (7.125 g) and triethylamine (4.81 ml) in anhydrous dichloromethane (70 ml) at room temperature. After 4 days, the mixture was evaporated under reduced pressure and the residue purified by column chromatography over silica, eluding with ethyl acetate/isohexane (1:4) to give the sub-title compound (7.34 g) as a solid. MS (+ve APCI) 346/348/350 ((M+H)+).

In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles, 7411-23-6, other downstream synthetic routes, hurry up and to see.

Reference:
Patent; Bantick, John; Ingall, Anthony; Perry, Matthew; Reynolds, Rachel; US2004/14634; (2004); A1;,
1,2,3-Triazole – Wikipedia,
Triazoles – an overview | ScienceDirect Topics