Research speed reading in 2021. Redox catalysis has been broadly utilized in electrochemical synthesis due to its kinetic advantages over direct electrolysis. 217448-86-7, name is Methyl 1-(2,6-difluorobenzyl)-1H-1,2,3-triazole-4-carboxylate belongs to triazoles compound, it is a common compound, a new synthetic route is introduced below. 217448-86-7
ExampIe-4: Preparation of l-(2, 6-difIuorobenzyl)-lH-l, 2, 3-triazole-4- carboxylic acid[0029] A mixture of Methyl l -(2, 6-difluorobenzyl)-l H- l, 2, 3-triazole-4- carboxylate. (50 gms) and a solution of sodium hydroxide ( 1 1.76 gms in 100ml water) were stirred at room temperature contents till it becomes clear. Hydrochloric acid (30ml) in DM water (70 ml) was charged to above reaction mass. Adjusted the PH of the reaction till 2-3 by adding the hydrochloric acid solution at 25-30C. After the completion, reaction mass was filtered and dried the material at 65C-70C for 15 hours. Yield: 40gms Example
Balanced chemical reaction does not necessarily reveal either the individual elementary reactions by which a reaction occurs or its rate law. In my other articles, you can also check out more blogs about 217448-86-7, and we look forward to future research findings.
Reference:
Patent; DAVULURI, Ramamohan Rao; WO2012/25936; (2012); A2;,
1,2,3-Triazole – Wikipedia,
Triazoles – an overview | ScienceDirect Topics